Can't enable iPod hard disk

I am trying to enable my 30GB iPod to be used as a hard disk to save documents. When I initially plug my iPod into my Mac, the iPod icon appears briefly on the desktop, then disappears.
Then, when I try to select "Enable Disk Use" on the iPod Summary page, I get the message "Waiting for iPod..." for about a minute, followed by "The settings were not saved for the iPod because it could not be found."
The funny thing is, when I used my iPod as a hard disk in the past it worked fine. But ever since I upgraded to iTunes version 7.0.2, it started giving me this error message and I have been unable to use my iPod as a hard disk ever since.

I haven't seen this problem since iTunes 6 and even then I was never able to find a complete answer to the "Preferences not saved" error as it was called then or any knowledge base articles with an official explanation. I did however find a workaround in a previous discussion but I don't know how if you could get it to work with iTunes 7. It involved connecting your iPod and in the short time that it was still visible on the desktop just as iTunes is opening, going to Preferences>iPod and ticking "enable disk use". You had to be quick but it could be done. In iTunes 7 it would mean quickly clicking on the iPod icon in the source list to bring up the Summary tab so you could enable disk use while the iPod was still showing on the desk top.
The only other suggestion I would have is to try restoring your iPod. restoring will erase the iPod's hard drive, reload the software and put it back to default settings, so if you have songs on your iPod that aren't on iTunes you will lose them if you have no back up. Once the restore is complete follow the on screen instructions and it should connect to iTunes and give you a prompt to automatically update your library onto the fresh installation. If you choose no it will default to manual mode which will default "enable disk use" and from there you can choose whatever setting you like: Restoring iPod to factory settings with iTunes 7

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