Disk Utility: "Repairing disk failed with error Could not unmount disk"

Disk Utility: “Repairing disk failed with error Could not unmount disk”
Hi. I’ve been experiencing some mildly squirrelly behaviour with my system (vide infra) so decided to repair the two internal hard drives on my computer. The primary hard drive is a 74.53 GB ST380013AS that came with the system; its S.M.A.R.T. Status is “verified” and Disk Utility repairs permissions just fine. However, the second internal drive (Maxtor 6L250S0, 233.76 GB, lower Bay, Journaled HFS+), despite being verified by S.M.A.R.T. status and apparently running OK, fails to unmount when I ask Disk Utility to repair it- I get the above error message in red. I have repaired this disk with DiskWarrior (v3.03) and all appears to run AOK. Can anyone tell me why I cannot get Disk Utility to run on this secondary (eg, non-startup) disk? I have tried many times and the error is reproducible. Thank you!
G5 1.6GHz PPC, 1 GB RAM, running OS 10.4.6

Thank you for these useful links!
For others who have this issue, I also found very helpful advice given to this question on the MacFixIt forums by MicroMat Tech3 at
http://www.macfixitforums.com/php/showthreaded.php?Cat=&Board=tiger&Number=76265 1
He said: "Use the lsof command to find the open files on a volume that does not unmount or eject. Open Terminal, located in /Applications/Utilities. Type: sudo lsof | grep Leave a space after the p in grep, then drag the icon of the problem volume to the Terminal window. The pathname for the volume is pasted in for you; press Return. Then enter your administrative password at the prompt, and press Return."
At this point, one now has a list of the open files/processes on the volume that will not unmount. You can use Activity Monitor to terminate these processes if you wish, and then the volume will unmount as it should.

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    In Finder's Menu, select Go menu>Go to Folder, and go to "/volumes". (no quotes)
    Volumes is where an alias to your hard drive ("/" at boot) is placed at startup, and where all the "mount points" for auxiliary drives are created for you to access them. This folder is normally hidden from view.
    Drives with an extra 1 on the end have a side-effect of mounting a drive with the same name as the system already think exists. Try trashing the duplicates with a 1 or 2 if there are no real files in them, and reboot.
    If it does contain data...
    http://support.apple.com/kb/TS2474

  • Could not unmount disk

    I am trying to do a clean install from Snow Leopard DVD disk to Macbook Pro. The computer stopped responding and after a restart I got a gray screen with a folder and ?. I have tried 3 different hard drives that have all been used in this MacBook Pro and all installed with Mountain Lion.I have zeroed out one hard drive using Disk Utility and I continue to get failed install. I cannot repair, partition, or erase any drive: Could Not Unmount Disk error on the computer using Disk Utility. I did all repairs using a separate iMac's Disk Utility. The computer is late 2009 Intel MacBook Pro. Please help

    pkj0192 wrote:
    The computer stopped responding and after a restart I got a gray screen with a folder and ?.
    All that says is the firmware can't find the bootable OS it was assigned to. Which you obviously erased.
    Hold the option/alt key at boot gives Startup Manager, which you then can select a new/other OS to boot from and set it as the startup disk in System Preferences.
    I have tried 3 different hard drives that have all been used in this MacBook Pro and all installed with Mountain Lion. I have zeroed out one hard drive using Disk Utility and I continue to get failed install.
    I assume you have used the 10.6 Disk Utiltiy and selected the ENTIRE drive, format Option: MBR and MSDOS, then click Erase and Security Option Zero All Data, and then go back to Partition 1: Option GUID and Format: OS X Extended J?
    This rebuilds the GUID and EFI so it's  for 10.6 version and removes all partitions on the drive, including the hidden RecoveryHD partition.
    I cannot repair, partition, or erase any drive: Could Not Unmount Disk error on the computer using Disk Utility. I did all repairs using a separate iMac's Disk Utility. The computer is late 2009 Intel MacBook Pro.
    If you have the drives hooked up to the iMac, Spotlight might be trying to index them thus they can't be unmounted. So have Spotlight ignore everything, turn it off basically.
    You can force unmount a drive in Terminal.
    ..Step by Step to fix your Mac
    Are you using the 10.6 white retail disk? Because that's what you need to boot/use on the 2009 MBP, not the iMac's 10.6 disk as those contain machine specific drivers for the iMac only. Don't format the drives on the iMac unless it's also 10.6.
    Since your issue appears on three drives, either there is a problem with the machine/cable or perhaps a bad 10.6 disk or wrong methods being used each time.
    How to erase and install Snow Leopard 10.6

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