How do I turn HD settings off to sync to ipod nano?

I have a 5th Generation iPod nano, and I recently purchased an episode of "Doctor Who", but apparently it won't sync to my ipod. I begin to figure its the HD setting and I have tried to turn it off using the playback option in prefences and set it to Standard Mode, but it still won't let me sync it?
Please help?

To turn it completely off, press and hold the Sleep/Wake button for a few seconds until the red "slide to power off" slider appears, and then slide the slider.
Regards.

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