Invisible files (??) blocking space on external hard disc

After using a dos formatted external hard disc with my Mac I can no longer save anything onto the free space with my PC. The is supposed to be at least 80 GB in that partition and both the Mac and the PC say the space is free. The Mac can save files onto it but not the PC. I have tried cleaning it on both systems but apart from doing a reformatting (lots of work to move the other content) does anyone have any more ideas? What hat the Mac put there that is invisible? I already deleted the Mac trash file (.$something) which was invisible on the PC. Now no files are showing up anywhere.

I definitely lost the Photos that I synced - not sure if it's because I saw the ! next to the AppleTV device in iTunes and selected it to see why, resulting in a sync without the connected photos - thus deleting those that were on the AppleTV originally.
I think this may be the case.
I haven't actually tested the effects of removing the external HD, but I've rather suspected that if it should become unavailable that the content of the tv would be safe, although I have also suspected it might be quite easy to force a sync without realising what was happening and thereby delete the content from the tv.
Of note, there have been numerous occasions over the last few months where my drive has been disconnected and I haven't given my tv syncing a thought and as yet I haven't lost anything.
The position I suspect will be quite different if I wanted to sync something on my mac while my HD is unavailable, I'm fairly sure I would delete everything from the tv. I believe the answer to the OP's question depends entirely on what they will be doing while the drive is disconnected.

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