IPod won't sync my new tv episode

The 10th tv episode of a show I purchased has been added to my iTunes account.
I want to sync my iPod with my iTunes in order to add the 10th episode (the other 9 are already on the iPod and there is still room for the 10th).
Wifi is off on the iPod.
I plugged my iPod into the usb on my Mac
Check what episodes I wanted on my iPod and hit sync. The circular arrows were spinning on my iPod but the new episode did not show up.
I also tried to manually click and drag the new episode to the iPod as per the instructions on iTunes Help with no success.
Any suggestions?
Thanks
T.

I should mention that I had an iPod that stopped working and then I got a new battery at the Apple store and everything was syncing perfectly.
Thank you.     

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