Manually added tracks put my iPhone over capacity. Now I can't sync. Help!

I have a number of Audiobook I tried to sync to my phone.  I could not find anywhere in the iPhone settings to choose to sync these (anyone know where?).  So I manually added them by dragging them from iTunes onto the iPhone. 
However they are very large files and put my iPhone "over capacity".  Now whenever I try to sync I get an error message saying:
"The iPhone “Mr Shiney” cannot be synced because there is not enough free space to hold all of the selected items (additional 7.38 GB required)."
But I can't unselect these files!  They don't appear in the "Manually Added Songs" section of the Music tab.  My phone is stuck in this weird state where I can no longer sync.
I have tried deleting the songs from iTunes.  But this now just says the songs couldn't be found so I still can't sync.
Should I restore from backup?  Won't I lose all my app content?  Any ideas what to do?
My iPhone is a 3G on iOS 4.2.1. iTunes is 10.5.

Have you touched the "More" button (on the iPhone).
then gone to Audio Books.
Are they there?
I had an audio book still on my iphone, it survivedf the iOS5 update.
To get rid of it, I plugged iPhone into Mac,
Go to itunes.
Click on Iphone in iTunes.
Go to Books tab,
Scroll down, there is audio books.
Choose sync selected audio books,
And untick the ones I don;t want.
Dows this work for you?

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