Export quality troubles

Please help how to make a good quality movie file after export.
I just would like to understand which export options I should choose to make it optimal (minimum quality loss and normal file size).
I've tried many options including even 'no compression' quicktime .mov file. In the last example I got 67 Gb 'black screen + sound' file for 12-minute film. The same with DV, however, the file was not so big.
h264, avi and some others - I've chosen best quality possible, but the result is too vague.
It's too long to try all the options possible, please give a wise counsel.
Second problem: after export I hear sounds which I don't (and should't) hear in the project and vice versa: I don't hear in the exported result what I hear in the project. Audio panel is detached, video and audio are fine in the project, but results are unacceptable.
Third problem: iMovie'11 sometimes does not register micro-level audio adjustments when I play a piece to check the result, I can't hear what I've made until the program is simply reopened.
What can be done?
Many thanks

when I play these .mov files separately (whether in actual size or fullscreen), they look quite acceptable, not DV/HD, but better than the result (you can check how it looks, http://vimeo.com/16457205)
I don't expect them to look better than they are after export, I just want not to loose at least this fair to middling quality. Is it a deadlock actually?

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